Nikolai I. Lisov, Valerii P. Sazonov Solubility, Solubility data series The synthetic method was used. The critical separation temperatures were determined by visual observation of the appearance of a meniscus. Critical temperatures determined in separate closed tubes and in the viscometers agreed within experimental error. Solutions were prepared from weighed amounts of the pure components. All manipulations were carried out in a dry box to eliminate contamination by moisture. The International Union of Pure and Applied Chemistry Stein, A.; Allegra, J. C.; Allen, G. F.; J. Chem. Phys. 55, 4265-9 (1971). paper https://doi.org/10.1063/1.1676745 79-24-3 1 C2H5NO2 InChI=1S/C2H5NO2/c1-2-3(4)5/h2H2,1H3 MCSAJNNLRCFZED-UHFFFAOYSA-N 75.0666 Nitroethane Purified by double distillation and by preparative gas chromatography; purity 99.97 mole% by GLC. 96-14-0 2 C6H14 InChI=1S/C6H14/c1-4-6(3)5-2/h6H,4-5H2,1-3H3 PFEOZHBOMNWTJB-UHFFFAOYSA-N 86.1754 3-Methylpentane Phillips; research grade; purity 99.99 mole%. Nitroethane with 3-Methylpentane