Components:

(1) 1,1,2,2-Tetrabromoethane, C2H2Br4; [79-27-6] NIST WebBook
(2) Water, H2O; [7732-18-5] NIST WebBook

Original Measurements

Blumberg, R.; Melzer, P.; TBE Bull. 2, 5 (1960).

Variables:

Ambient temperature: 302 - 324 K

Prepared by:

A.L. Horvath

Method/Apparatus/Procedure:

The only available information refers to the determination of water in the organic phase by the Karl Fischer titration method. The overall experimental error was about ñ 20 %.

Source and Purity of Materials:
  1. Source and purity not given.
  2. Distilled (compiler).
Estimated Errors:

Ambient temperature: ±1 K.
Mass concentration (m/v) (1): See table above.

Experimental Values:
T (°C) w1 100w2 x1 x2
29.0 - 4 x 10-2 - 7.62 x 10-3
51.0 3.0 x 10-1 1.5 x 10-1 1.57 x 10-4 2.80 x 10-2

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