Components:

(1) 2,3-Dichloro-1,3-butadiene, C₄H₄Cl₂; [1653-19-6] NIST WebBook
(2) Water, H₂O; [7732-18-5] NIST WebBook

Original Measurements

Vojtko, J.; Hrusovsky, M.; Kanala, A.; Chemicke Zvesti, 21, 443 (1967)

Variables:

Ambient temperature: 293 K

Prepared by:

A.L. Horvath

Method/Apparatus/Procedure:

The titration method as described elsewhere¹ was used. Solubility data for the ternary system of water-methanol-2,3-dichloro-1,3-butadiene were also reported.

Source and Purity of Materials:

1. Synthesis was described elsewhere.₂ At 20°C, n_D =1.4887 and d₄ = 1.1838 g/cm³.
2. Distilled.

Estimated Errors:

Ambient temperature: ±1.0 K (compiler).
Mass concentration (m/v) (1): Not specified.

References

¹ Othmer, D. F.; White, R. E.; Trueger, E.; Ind. Eng. Chem. 1941, 33(10), 1240-8.
² Carothers, W. H.; Berchett, G. J.; J. Am. Chem. Soc. 55, 2004 (1933).