Components:

(1) Nitroethane, C₂H₅NO₂; [79-24-3] NIST WebBook
(2) 1-Nitropropane, C₃H₇NO₂; [108-03-2] NIST WebBook
(3) 2-Nitropropane, C₃H₇NO₂; [79-46-9] NIST WebBook
(4) Oil fraction of Tuimazin crude, None; [mix-06] NIST WebBook

Original Measurements

Pol'shinskii, V. V.; Kozlov, L. M.; Chem. Technol. Fuels Oils 1970, 6(10), 730-734.

Variables:

Ambient temperature: 255 - 334 K

Prepared by:

N.I. Lisov, V.P. Sazonov

Method/Apparatus/Procedure:

The method, described in Bondarev and Kozlov¹ was used. No experimental details given.

Source and Purity of Materials:

1. Obtained by nitration gas distillate; contained 23 vol.% nitroethane, 48.7 vol.% 1-nitropropane and 28.3 vol.% 2-nitropropane; n(20°C,D) = 1.3975; d(20°C, 4°C) = 1.0088.
2. Obtained by nitration gas distillate; contained 23 vol.% nitroethane, 48.7 vol.% 1-nitropropane and 28.3 vol.% 2-nitropropane; n(20°C,D) = 1.3975; d(20°C, 4°C) = 1.0088.
3. Obtained by nitration gas distillate; contained 23 vol.% nitroethane, 48.7 vol.% 1-nitropropane and 28.3 vol.% 2-nitropropane; n(20°C,D) = 1.3975; d(20°C, 4°C) = 1.0088.
4. Obtained by distillation of Tuimazin crude between 440 and 520°C; stocks obtained by division of oil fraction on silica gel by liquid chromatography

Estimated Errors:

Ambient temperature: Not specified.
Mass concentration (m/v) (1): Not specified.

References

¹ Bondarev, S. V.; Kozlov, L. M.; Chem. Technol. Fuels Oils 4(10), 720-724 (1968)