SDS Volume (4975)

Volume 77. Nitroalkanes with Water or Organic Solvents: Binary and Multicomponent Systems, p 50

Original Measurements

Vreeland, J.; Dunlap, R.; J. Phys. Chem. 61, 329-33 (1957).

Variables:

Temperature: 298 K

Prepared by:

N.I. Lisov, V.P. Sazonov

Method/Apparatus/Procedure:

No experimental details given.

Source and Purity of Materials:
  1. Matheson Chemical Co.; research grade; distilled through a Todd column; b. p. = 114.7°C - 114.8°C.
  2. Minnesota Mining and Manufacturing Co.; distilled; b. p. = 178.8°C - 179.1°C.

Nitroethane with Heptacosafluorotributanamine

Components:

(1) Nitroethane, $\ce{ C2H5NO2 }$; [79-24-3] NIST WebBook
(2) Heptacosafluorotributanamine, $\ce{ C12F27N }$; [311-89-7] NIST WebBook

Experimental Values:

The solubility of nitroethane (1) in heptacosafluorotributanamine (2) at 298 K was reported to be 100 w1 = 0.1.
The corresponding mole fraction, x1, calculated by the compilers is 0.009.
The solubility of heptacosafluorotributanamine (2) in nitroethane (1) at 298 K was reported to be 100 w2 = 0.1.
The corresponding mole fraction, x2, calculated by the compiler is 0.0001.

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