SDS Volume (4864)
Volume 77. Nitroalkanes with Water or Organic Solvents: Binary and Multicomponent Systems, p 72
Original Measurements
Warner, R. K.; Aust. J. Appl. Sci. 4, 581-9 (1953).
Variables:
Temperature: 293 K
Prepared by:
Method/Apparatus/Procedure:
The analytical method was used. (2) was placed with the appropriate amount of pure (1) in a small flask. The contents of the flask were warmed to 30 to 50 °C, agitated with excess (2) for 15 min, and then placed in a constant temperature bath at 20 °C with intermittent shaking for 6 to 8 h. Crystallization from the supersaturated solution occurred, and when equilibrium was reached the solution was quickly decanted, filtered to remove the fine crystals, and placed in a stoppered flask at 20 °C before analysis.
Source and Purity of Materials:
- Synthesized by standard method; thoroughly dried and fractionally distilled.
- Source not specified; A. R. grade; not purified.
Nitroethane with Uranyl nitrate hexahydrate
Components:
(1) Nitroethane,
$\ce{ C2H5NO2 }$;
[79-24-3]
NIST WebBook
(2) Uranyl nitrate hexahydrate,
$\ce{ UO2(NO3)2(6H2O) }$;
[13520-83-7]
NIST WebBook
Experimental Values:
The solubility of uranyl nitrate (2) in nitroethane (1) at 293 K was reported to be 100 w2 = 5.1.
The corresponding mole fraction, x2, calculated by the compiler is 0.010.
